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Córdoba Province in Argentina is a global hotspot for deep hail-producing storms. Previous studies of hail formation and detection largely relied on satellite snapshots or modeling studies, but lacked hail validation, relying instead on proxy metrics. To address this limitation, this study used hail collected in the mountainous Córdoba region in collaboration with the citizen science program “Cosecheros de Granizo 2018–2020” including from a record-breaking hail event and from the 2018–2019 RELAMPAGO field campaign. Three cases including a MCS and two supercells, which have verified hail in different environment locations relative to the Sierras de Córdoba, were analyzed for multi-spectral signatures in GOES-16 satellite data. Brightness temperatures decreased over time after convective initiation, reaching values cooler than the tropopause with variations around those values of different magnitudes. Overall, all cases exhibited a slight weakening of the updraft and strong presence of smaller ice crystal sizes just prior to the hail report, especially for the larger hailstones. The results demonstrate promise in using satellite proxies for hail detection in multiple environments for different storm modes. The long-term goal is to better understand hail-producing storms and unique challenges of forecasting hail in this region.